@Zanchet_UNICAMP@LatinXChem@nanoscale_rsc@beyondbenign@green_rsc@RSC_Sus Hi Daniela, thank you for the interest in my work. Answering your question, most of the methodologies found for the elaboration of W/O nanoemulsions use a long time of ultrasonication, besides using high levels of energy and even use high homogenization periods,
@NanoGoch@LatinXChem@nanoscale_rsc@beyondbenign@green_rsc@RSC_Sus 2) Other characterization techniques we can use are scanning electron microscopy (SEM), atomic force microscopy (AFM), nuclear magnetic resonance spectroscopy (NMR) and infrared spectroscopy (IR). In addition, physical tests such as viscosity and refractive index can be performed
@NanoGoch@LatinXChem@nanoscale_rsc@beyondbenign@green_rsc@RSC_Sus So, the DLS shown in the poster is of the majority part which is the yellow one. The DLS of the lower proportion fraction was not shown, but this emulsion shows a droplet size of about 16 nm, but we are still studying it.
@NanoGoch@LatinXChem@nanoscale_rsc@beyondbenign@green_rsc@RSC_Sus Hello Dr. Natalia, thank you for your interest in my work. Answering your questions:
1) To measure the nanoemulsion in the DLS is taken from the reaction mixture. We are obtaining two nanoemulsions in the mix, which are very easy to separate.