@uOttawaNMR You wouldn't still happen to have that hoesy dataset would you? I've been having the darnedest time getting a hoesy to work. Super low signal to noise. Having a working parameter set would be invaluable to me.
With our new 800 #NMR and NMR facility manager, this would be perfect for someone with interests in biophysical NMR. Reach out if you have questions! @nmr900
We have two positions at the associate/assistant level. One is focused on organic chemistry, the other is open. Come work with us! https://t.co/DYOEmuaJZO
@Popher@nmr900 Update: It seems to work. You need to modify the pulse program to include "SWITO" statements, and sometimes this involves adjusting delays to maintain phasing. Decoupling during acquisition is harmful to the SNR.
Is there any reason why a Bruker QNP accessory couldn't be used to collect phase-sensitive gradient experiments (e.g. a 19F{1H} HOESY on a 1H/BBF probe)? "hoesyfhqfqnrv" is okay, I'd like to clean up artifacts, and that program is limited to QF mode. @nmr900#NMR
@Popher@nmr900 I'm trying. I modified one of them to add the QNP switch commands. I think it's working, but I'm getting lower signal than expected. By default, those programs are not written for the QNP accessory, and it looks like they expect separate amplifiers for H and F.
Starting today, thanks to @NSF, MSU is now recycling nearly all of the helium in its #NMR facility. It's been a crazy week, but Bryan from @BlueFors_Ltd got us up and running. @nmr900
So, what would be on your list?
What promises do you want to make to yourself?
Use John Wooden's list as a spark, but create your own. Write them out and look at them at the start of every day.
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@PatrickLab_MS@RCSA1 "If you lose one sense, your other senses are enhanced. This is why people with no sense of humor have a heightened sense of self-importance." - the internet
Dan's looking for his next position, so please reach out if you need a creative and innovative scientist with expertise in protein biochemistry/biophysics, nanomaterials, and 3D printing!
A couple of days late, but congratulations to Dr. Dhanush Amarasekara for successfully defending his dissertation entitled "Engineering Functionalized Nanomaterials for Targeting and Ablating Biofilms."